Recovering Ga(III) from coordination complexes using pyridine 2,6-dicarboxylic acid chelation ion chromatography

K Staff; MB Brown; Robert Hider; Xiao Kong; P Friden; Stuart Jones

doi:10.1002/bmc.1402

Recovering Ga(III) from coordination complexes using pyridine 2,6-dicarboxylic acid chelation ion chromatography

K Staff, MB Brown, Robert Hider, Xiao Kong, P Friden, Stuart Jones

Institute of Pharmaceutical Science

Research output: Contribution to journal › Article › peer-review

10 Citations (Scopus)

Abstract

Ion exchange chelation chromatography is an effective means to extract metals from coordination complexes and biological samples; however there is a lack of data to verify the nature of metal complexes that can be successfully analysed using such a procedure. The aim of this study was to assess the capability of pyridine 2,6-dicarboxylic acid (PDCA) to extract and quantify Ga(III) from a range of environments using standard liquid chromatography apparatus. The PDCA chelation method generated a single Ga(III) peak with a retention time of 2.55 +/- 0.02 min, a precision of 15. Copyright (C) 2010 John Wiley & Sons, Ltd.

Original language	English
Pages (from-to)	1015 - 1022
Number of pages	8
Journal	Biomedical Chromatography
Volume	24
Issue number	9
DOIs	https://doi.org/10.1002/bmc.1402
Publication status	Published - Sept 2010

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title = "Recovering Ga(III) from coordination complexes using pyridine 2,6-dicarboxylic acid chelation ion chromatography",

abstract = "Ion exchange chelation chromatography is an effective means to extract metals from coordination complexes and biological samples; however there is a lack of data to verify the nature of metal complexes that can be successfully analysed using such a procedure. The aim of this study was to assess the capability of pyridine 2,6-dicarboxylic acid (PDCA) to extract and quantify Ga(III) from a range of environments using standard liquid chromatography apparatus. The PDCA chelation method generated a single Ga(III) peak with a retention time of 2.55 +/- 0.02 min, a precision of 15. Copyright (C) 2010 John Wiley & Sons, Ltd.",

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AU - Hider, Robert

AU - Kong, Xiao

AU - Friden, P

AU - Jones, Stuart

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N2 - Ion exchange chelation chromatography is an effective means to extract metals from coordination complexes and biological samples; however there is a lack of data to verify the nature of metal complexes that can be successfully analysed using such a procedure. The aim of this study was to assess the capability of pyridine 2,6-dicarboxylic acid (PDCA) to extract and quantify Ga(III) from a range of environments using standard liquid chromatography apparatus. The PDCA chelation method generated a single Ga(III) peak with a retention time of 2.55 +/- 0.02 min, a precision of 15. Copyright (C) 2010 John Wiley & Sons, Ltd.

AB - Ion exchange chelation chromatography is an effective means to extract metals from coordination complexes and biological samples; however there is a lack of data to verify the nature of metal complexes that can be successfully analysed using such a procedure. The aim of this study was to assess the capability of pyridine 2,6-dicarboxylic acid (PDCA) to extract and quantify Ga(III) from a range of environments using standard liquid chromatography apparatus. The PDCA chelation method generated a single Ga(III) peak with a retention time of 2.55 +/- 0.02 min, a precision of 15. Copyright (C) 2010 John Wiley & Sons, Ltd.

U2 - 10.1002/bmc.1402

DO - 10.1002/bmc.1402

M3 - Article

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ER -

Recovering Ga(III) from coordination complexes using pyridine 2,6-dicarboxylic acid chelation ion chromatography

Abstract

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